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Synlett 2000; 2000(10): 1439-1442
DOI: 10.1055/s-2000-7658
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Stereoselective Synthesis of (E)-β-Arylvinyl Halides by Microwave-Induced Hunsdiecker Reaction

Chunxiang Kuang* , Hisanori Senboku, Masao Tokuda
  • *Division of Molecular Chemistry, Graduate School of Engineering, Hokkaido University, Sapporo 060-8628, Japan; Fax + 81-11-706-6598; E-mail: tokuda@org-mc.eng.hokudai.ac.jp
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Publication Date:
31 December 2000 (online)

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(E)-β-Arylvinyl halides were prepared in high yields in a short reaction (1-2 min) by microwave irradiation of the corresponding 3-arylpropenoic acids in the presence of N-halosuccinimide and catalytic LiOAc.

haloalkenes - α,β-unsaturated carboxylic acid - stereoselective synthesis - microwave irradiation - Hunsdiecker reaction

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