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Synlett 1995; 1995(12): 1280-1282
DOI: 10.1055/s-1995-5256
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Stereoselective Synthesis of Methylenephosphonate Analogues of 2-Deoxyribose 3-Phosphates through Cyclization of Alkyl Radicals to Vinylphosphonates

Tsutomu Yokomatsu, Takanori Shimizu, Yoko Yuasa, Shiroshi Shibuya*
  • *School of Pharmacy, Tokyo University of Pharmacy and Life Science, 1432-1 Horinouchi, Hachioji, Tokyo 192-03, Japan
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Publication Date:
31 December 2000 (online)

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Methylenephosphonate analogues of 2-deoxyribose 3-phosphate were efficiently synthesized in a highly diastereoselective manner (>92% de) through intramolecular addition of a radical to vinylphosphonates.

2-deoxyribose 3-phosphates - methylenephosphonate analogues - radical cyclization - vinylphosphonates

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