Synfacts

Ausgabe 12 · Dezember 2022

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Ausgabe
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A183
SYNFORM ISSUE 2022/12 FREIER ZUGRIFF

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Synthesis of Natural Products
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1277
Synthesis of (–)-Bufospirostenin A

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1278
Enantioselective Total Synthesis of (+)-Lucidumone

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1279
Total Synthesis of (±)-Rameswaralide FREIER ZUGRIFF

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1280
Synthesis of (±)-2‑Isocyanoallopupukeanane

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1281
Synthesis of (±)-Resiniferatoxin

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1282
Total Synthesis of (±)-Ginkgolide C

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1283
Total Synthesis of (±)-Saxitoxin FREIER ZUGRIFF

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Synthesis of Heterocycles
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1285
Silver-Free Chemoselective O-Benzylation of 2‑Quinolinones

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1286
Phase Dependent Tautomerism of 1,3-Thiazine Derivatives

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1287
Synthesis of N-Heterocycles via Photoredox Catalysis using Bifunctional Sulfilimines and Alkenes

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1288
Skeletal Editing through Nitrogen Atom Insertion to Indoles

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1289
Synthesis of Cyclic Enecarbamates through Dehydrogenation

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1290
Pd-Catalyzed Synthesis of 2,4-Diarylthiazoles

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1291
Synthesis of N^β‑Substituted 1,2-Diazetidin-3-ones

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1292
Metal- and Photocatalyst-Free Switchable Redox Photoexcited Annulation of 2-Nitroarylethanols to NHCs

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1293
Oxidative Nucleophilic Substitution of Hydrogen for the Synthesis of Aminated Nitro-Substituted Heteroarenes

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1294
One-Pot Multicomponent Protocol To Access Sulfenylimidazo[1,5‑a]pyridines

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1295
Synthesis of Aziridines by Reaction of Free Amines with Alkenylthianthrenium Salts

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1296
Oxidative Condensation to Access Quinoxalines

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1297
Diastereoselective Synthesis of THF Derivatives

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Synthesis of Materials and Unnatural Products
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1299
Modular Syntheses of Defined Graphene Nanoribbons FREIER ZUGRIFF

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1300
New Synthesis of Mesodiphenylhelianthrene with Its Endoperoxide Formation

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1301
Pleiadienes from Palladium-Catalyzed [5+2] Annulation

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1302
Magic Graphyne Wheel

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1303
Unexpected Cascade Leading to δ-Carboline

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1304
Economical Metal-Free Heterocycle Arylation

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1305
Ladder Fluorenylidenefluorene Oligomers

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1306
Tetracyclic Heteroaromatics from Isocyanide Insertion

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1307
Polyselenophenes from Elemental Selenium

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1308
Electrophile-Modulated Regiodivergent Syntheses

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1309
‘Bottom-Up’ Synthesis of a Semibuckminsterfullerene

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1310
Superhelicene with NIR Circularly Polarized Emission

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Metals in Synthesis
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1311
Nickel-Catalyzed Enantioselective Multicomponent Reaction of 1,3-Dienes, Aldehydes, and Boronic Acids FREIER ZUGRIFF

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1312
Enantio- and Regioselective Hydroalkenylation of Alkenes with Enamides under Iridium Catalysis

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PDF (89 kb)
1313
Introducing the Magic Methyl: Enantioselective Hydromethylation of Olefins under Copper Hydride Catalysis FREIER ZUGRIFF

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1314
Organolanthanide-Catalyzed α-Borylation of Pyridines: Metal Size Controls Product Distribution

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1315
Rhodium-Catalyzed Directed C–H Activation–Insertion Cascade Using Vinylene Carbonate

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1316
Asymmetric Hydrogenation of E/Z-Olefin Mixtures by Cobalt Catalysis

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1317
Palladium-Catalyzed Annulations Towards π-Extended Coumarins

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1318
Palladium-Catalyzed Tandem Aza-Heck Cyclization/C(sp³)–H Functionalization

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1319
Iridium-Catalyzed Asymmetric Alkylation of Cyclic Alkenes Using N-Methyl-2-Aminopyridines

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1320
Nucleophilic Addition of Benzylic and α-Heteroatom-Substituted Silanes to Aldehydes under Dual Catalysis

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1321
Iridium Photocatalyzed Fluoroalkenylation Reaction of Alkyl-Tethered Alkynes

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1322
Dual Tungsten/Copper Photocatalysis Enables Direct C(sp³)–H Allylation of Alkanes with Allylic Chlorides

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1323
Copper-Mediated Regio- and Diastereoselective Synthesis of Polysubstituted Spiropentanes

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1324
Palladium(II)-Catalyzed Domino Cacchi/C–H Activation/Arene Insertion Sequence

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1325
Enantioselective Aziridination of Alkenes Utilizing a C₄-Symmetric Dirhodium(II) Catalyst

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1326
Enantioselective Synthesis of Tetrahydrofurans via a Palladium-Catalyzed [3+2] Cycloaddition

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1327
Nickel-Catalyzed Intramolecular Carbo-Oxygenation of Alkenes Using N₂O as the Oxygen Source

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1328
Direct Arylative Substitution of Homoallylic Alcohols with Arylboroxines under Nickel Catalysis

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PDF (66 kb)
1329
Iridium-Catalyzed Enantioselective Hydrogenation of Oximes under Lewis and Brønsted Acid Cooperation

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1330
Nucleophilic Substitution of Propargylic Alcohols with Arylboronic Acids by Gallium and/or Silver Catalysis

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1331
Atroposelective Suzuki–Miyaura Cross-Coupling of ortho-Sulfonyl-Substituted Aryls to Chiral Biaryls

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1332
Asymmetric Hydroalkylation of Cyclopropenes with Alkyl Iodides Enabled by Nickel–Hydride Catalysis

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1333
Mono- and Dicarboxylation of Unactivated Alkenes Enabled by Photocatalysis

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1334
Enantioselective Intermolecular Hydroselenation of Alkenes Using a Cationic Rhodium Catalyst

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1335
Access to Halogenated Benzofurans via Au(I)-Catalyzed Cyclization/Hydroarylation of o-Alkynylphenols

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1336
Radical Methylation of Primary and Secondary C(sp³)–H Bonds under Copper Catalysis

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1337
Molybdenum-Catalyzed Deoxygenative Homo-Coupling of Aromatic Carbonyl Compounds to (E)-Alkenes

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1338
Palladium-Catalyzed Silylation via a C–C Bond Cleavage of Unstrained Ketones

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1339
1,1,2,2-Tetraborylalkanes via Sequential Diborylation of Terminal Alkynes

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Polymer-Supported Synthesis
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1341
Decarboxylative Conjugate Addition of Carboxylic Acids with Alkenes on a Triazine Framework Photocatalyst

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1342
Arene Hydrogenation by Cooperative Catalytic Systems of Metal Nanoparticles and Lewis Acids

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1343
Photochemical Giese Reaction of Dioxolane and Vinyl Ketones on Graphitic Carbon Nitride FREIER ZUGRIFF

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1344
Cycloaddition of CO₂ with Epoxides and Knoevenagel Condensation on a Pb₁₀K₂ Organic Framework

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1345
Photochemical Azide–Alkyne Cycloaddition Catalyzed by a Cuprous Iodide-Based Coordination Polymer

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1346
Hydrogenation of Nitriles Promoted by Silica-Supported Nickel Nanoparticles

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1347
Aza-Henry Reaction and Oxidation of 1,2,3,4-Tetrahydroisoquinolines on a Copper Nanocatalyst

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1348
Iron Chloride Derived Nanoparticles Containing ppm Levels of Ligated Palladium for Negishi Coupling

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1349
Synthesis of Benzo[a]pyrano[2,3-c]phenazine Derivatives on CuO Quantum Dots

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PDF (108 kb)
1350
Zinc-Catalyzed Photochemical Dehydrogenative Cycloaddition and Carbonyl Cyanosilylation

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1351
Reductive Annulation of Quinolines and Enones on an Ir Catalyst Supported on Hierarchically Porous Zirconia

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Organo- and Biocatalysis
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1353
Halogen-Atom and Group Transfer Reactivity through Quantum Mechanical Tunneling

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1354
Biocatalytic Cascade Approach Permits Rapid Access to Enantioenriched 1,2-Amino Alcohols

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1355
Ene-Reductase Permits Cross-Electrophile Coupling of α-Chloro Carbonyls with α-Aryl Nitroalkanes FREIER ZUGRIFF

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1356
Photocatalytic Amidylimination of Terminal Alkenes

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1357
Noncovalent Interactions Tame Radical Intermediates

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1358
Organophotocatalytic Generation of Alkyl Radicals by C–C Bond Cleavage and Radical Conjugate Addition

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1359
Direct Photocatalytic Reductive Benzoylation of Olefins with Benzoic Acids

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1360
Electrophotocatalytic Formation of Regioisomeric Oxazolines from Aryl Olefins

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1361
Hydrosilane Organocatalyst Permits Broadly Applicable Amidation under Mild Conditions

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1362
NHC-Catalyzed Atroposelective Synthesis of 1,3-Oxazepine-Containing Bridged Biaryls

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1363
Thioxanthone/TfOH-Photocatalyzed Xylene-Mediated Hydrogenation of α,β-Unsaturated Carbonyls

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1364
Skeletal Editing of Aryl Azides toward Aminopyridines through Nitrogen Insertion and Carbon Deletion

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Innovative Drug Discovery and Development
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1365
RapaBlock, a Novel Drug that Prevents the On-Target – Off-Tissue Effects of mTOR Inhibition

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1366
Small Molecule Inhibitors of the YAP-TEAD Interaction FREIER ZUGRIFF

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1367
The Fabulous Fabimycin

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1368
From Data to Prediction: Thermal Risk Analysis of Cyclic Sulfamidates

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1369
Discovery of a Potent Importin Inhibitor for Cancer Treatment

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1370
Nanogels with Cyanine Cross-Linker Enable Light-Mediated Control of Drug Delivery and Release

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1371
Discovery of a Next-Generation Inhibitor of HIV-1 Maturation Based on Betulinic Acid

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1372
Total Synthesis of Elongation Factor Antagonist SR-A3

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PDF (87 kb)
1373
Poxin-Resistant cGAMP-Derivatives Halt Viral Escape

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1374
Janustatins – Cytotoxic Polyketide Alkaloids

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1375
Efficient Synthesis of SM-406

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PDF (111 kb)
1376
A Versatile Approach Towards Novel Pleuromutilin Antibiotics

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1377
Synthesis of Coagulation Factor Xa Inhibitor Apixaban FREIER ZUGRIFF

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Peptide Chemistry
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1379
Domino Reaction to Form Polycyclic Spiro Compounds Containing Amino Acid Residues

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1380
Nickel/Iridium-Catalyzed Cross-Coupling of Amino Acid Chlorides with C(sp³)–H Hydrocarbons

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PDF (68 kb)
1381
Photoredox Cobaloxime/Iridium Complex-Catalyzed Peptide-Bond Formation FREIER ZUGRIFF

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PDF (116 kb)
1382
Microwave-Induced Inverse Peptide Synthesis

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PDF (70 kb)
1383
Copper-Catalyzed Alkynylation of Azapeptides

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PDF (65 kb)
1384
Zinc-Catalyzed Desymmetric Reduction To Form Hydroxylated Tetrasubstituted Amino Acids

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1385
Electrochemical Tandem Azidation/Heterocyclization of Tryptophan-Containing Peptides

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1386
Synthesis of N-Allyl Amino Acids and Peptides FREIER ZUGRIFF

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Flow Chemistry
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1387
Development of Continuous Flow System for β-Keto Ester Synthesis

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1388
Synthesis of Unsymmetrical Biaryls via Photoinduced Arylation of Chloroarenes in Flow

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PDF (70 kb)
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