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Synlett 2001; 2001(9): 1476-1478
DOI: 10.1055/s-2001-16806
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Efficient Synthesis of EDO-S,S-DMEDT-TTF, a Potent Organic-Donor for Synthetic Metals

Takako Konoike* , Kosuke Namba, Tetsuro Shinada, Kazuhiko Sakaguchi, George C. Papavassiliou, Keizo Murata, Yasufumi Ohfune
  • *Department of Material Science, Graduate School of Science, Osaka City University, Sugimoto, Osaka 558-8585, Japan; Fax + 81(0)6-6605-3153; E-mail: ohfune@sci.osaka-cu.ac.jp
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Publication Date:
28 August 2001 (online)

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Optically active ethylenedioxy-S,S-dimethylethylenedithiotetrathiafulvalene (EDO-S,S-DMEDT-TTF: 1) has been synthesized in satisfactory yield using a triethyl phosphite-mediated cross-coupling of (5S,6S)-5,6-dimethyl-1,3-dithiolane-2-one 4 with unsubstituted 1,3-dithiolane-2-thione 6.

organic-donor - EDO-DMEDT-TTF - 1,3-dithiolane-2-thione - cross-coupling

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