Synlett

Category: addenda and errata

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Issue 08/2012

Concise Formal Synthesis of (+)-Englerin A and Total Synthesis of
(-)-Orientalol F: Establishment of the Stereochemistry of the Organocatalytic [4+3]-Cycloaddition Reaction

Issue 04/2012

Organoselenosilane-Mediated Selective Mild Access to Selenolesters,
Selenoanhydrides and Diacyl Diselenides
Dual Activation in Organocatalysis: Design of Tunable and Bifunctional
Organocatalysts and Their Applications in Enantioselective Reactions

Issue 03/2012

Facile N-Urethane-Protected α-Amino/Peptide Thioacid Preparation Using EDC and Na2S
The Wieland-Miescher Ketone: A Journey from Organocatalysis to Natural Product Synthesis

Issue 01/2012

Enantioselective Intramolecular Hydroamination of N-Alkenyl Ureas
Catalyzed by tropos BIPHEP-Gold(I) Complexes with Au-Au Interaction

Issue 19/2011

In Situ Generation of Palladium Nanoparticles: Reusable, Ligand-Free Heck Reaction in PEG-400 Assisted by Focused Microwave Irradiation
A Highly Sustainable and Active Catalyst for Suzuki-Miyaura Reaction:
Palladium-Supported Ionic Liquid Catalyst (SILC) Coated with Polymer
Synthesis of Aminoindolizine and Quinoline Derivatives via Fe(acac)3/TBAOH-Catalyzed Sequential Cross-Coupling-Cycloisomerization Reactions

Issue 18/2011

The Hieber Anion [Fe(CO)3(NO)]-

Issue 17/2011

Synthesis of the Hypoxic Signaling Inhibitor Furospongolide

Issue 15/2011

Synthesis of Urea and Carbamate Glycosides Employing Unprotected Carbohydrates
An Inverse Electron-Demand Diels-Alder-Based Total Synthesis of Urolithin M7

Issue 14/2011

Perhydroazulenes - A New Class of Liquid Crystalline Materials
Sodium Dithionite

Issue 12/2011

Perhydroazulenes - A New Class of Liquid Crystalline Materials
Diarylprolinol in the Direct Asymmetric Aldol Reaction of
Trifluoromethylacetaldehyde Ethyl Hemiacetal with Aldehyde

Issue 11/2011

A Green Chemistry Method for the Regeneration of Carbonyl Compounds from Oximes by Using Cupric Chloride Dihydrate as a Recoverable Promoter for Hydrolysis

Issue 09/2011

Highly Diastereoselective Construction of Substituted Pyrrolidines: Formal Synthesis of (-)-Bulgecinine
First Friedel-Crafts Reaction of the Baylis-Hillman Adducts Derived from
Nitroolefins: Application towards Synthesis of Pyrrolidines and
Spiropyrrolidines

Issue 08/2011

Chemoenzymatic Synthesis of Idesolide from Benzoic Acid

Issue 05/2011

Chiral Sodium Phosphate Catalyzed Enantioselective 1,4-Addition of TMSCN to Aromatic Enones

Issue 03/2011

A Short and Efficient Route from myo- to neo-Inositol

Issue 01/2011

Direct Conversion of Olefins into α-Bromo Ketones Using O-Iodoxybenzoic Acid and Tetraethylammonium Bromide

Issue 20/2010

Electrophilic Functionalization of Non-Activated Olefins Catalyzed by
Lewis Superacids
2-Bromoacetophenone

Issue 19/2010

Polymer-Supported α-Aminonitriles: Alkylation Reactions and Carbonyl Compound Cleavage

Issue 15/2010

Sodium Hydride

Issue 14/2010

Fluorous Mixture Synthesis of Four Stereoisomers of the C21-C40 Fragment of Tetrafibricin

Issue 13/2010

Synthesis of Novel Haptens and Conjugates for Antibody Production against Kainoid Family

Issue 12/2010

Stereocontrolled Synthesis of Enantiopure Polyhydroxylated Azetidines via 1,2-Oxazines
Two-Phase Terpene Total Synthesis: Historical Perspective and Application to the Taxol® Problem

Issue 11/2010

Editorial

Issue 10/2010

Efficient and Atom-Economic Synthesis of α-Substituted β-Chromonyl-α,β-unsaturated Carbonyls through Molecular Rearrangement

Issue 09/2010

Regioselective Reductive Ring Opening of Benzylidene Acetals Using
Triethylsilane and Iodine

Issue 07/2010

Design and Synthesis of an Activity-Based Probe Template for Protein Kinases

Issue 05/2010

Chemistry of Lactam-Derived Vinyl Phosphates: Stereoselective Synthesis of (+)-Fagomine
A Practical Synthesis of (S)-Cyclopent-2-enol

Issue 04/2010

Fluorous Mixture Synthesis of Four Stereoisomers of the C21-C40 Fragment of Tetrafibricin

Issue 03/2010

A Simple, Advantageous Synthesis of 5-Substituted 1H-Tetrazoles

Issue 02/2010

Carbon-Carbon Double-Bond Isomerization and Diels-Alder Reaction of
Dimethyl 5-Methylene-4-isopropylidene-2-cycloheptene-1,1-dicarboxylate with Dienophiles

Issue 01/2010

Synthesis of Functionalized p-Terphenyls Based on Site-Selective Suzuki Cross-Coupling Reactions of Bis(triflates) of 2,5-Dihydroxybenzoate

Issue 20/2009

Chemistry of 2-Arylhydrazonals
Biomimetic Oxidation of Alcohols Catalyzed by TEMPO-Functionalized
Polyethylene Glycol and Copper(I) Chloride in Compressed Carbon Dioxide

Issue 19/2009

A Novel, Practical Synthesis of Sulfonyl Chlorides from Thiol and Disulfide Derivatives
Sustainable Click Reaction Catalyzed by Supported Ionic Liquid Catalyst (Cu-SILC)
Organocatalytic Asymmetric Triple Domino Reactions of Nitromethane with α,β-Unsaturated Aldehydes

Issue 18/2009

Studies on the Base-Catalysed Addition of Amines to Alkynes and Allenes:
A Novel Cascade Sequence for the Construction of Spirocyclic Aminals
Diastereoselective Thia-Claisen Rearrangement of Pyrrolidinone-Derived
Ketene N,S-Acetals
Concise Asymmetric Total Synthesis of ent-Guadinomic Acid from an Epoxy Alkenol

Issue 17/2009

A Facile Access to Antiflu Agent Tamiflu/Oseltamivir

Issue 14/2009

A Novel Approach to Monobenzannulated Spiroketals Using Styrenes in the Kulinkovich Reaction
Enhancement of Enantioselection in the Copper-Catalysed Intramolecular Büchner Reaction by Variation of the Counterion

Issue 10/2009

Microwave-Assisted Rhodium-Catalyzed Decarbonylation of Functionalized 3-Formyl-2H-chromenes: A Sequence for Functionalized Chromenes like
Deoxycordiachromene

Issue 09/2009

Tandem Aza-Michael-Condensation-Aldol Cyclization Reaction: Approach to the Construction of DE Synthon of (±)-Camptothecin

Issue 08/2009

The Gold(I)-Catalyzed Cycloisomerization of 1,6-Enynes to 1,4-Dienes

Issue 05/2009

Burgess Reagent: From Oblivion to Renaissance in Organic Synthesis

Issue 02/2009

Synthesis of Chiral Carbohydrate Ionic Liquids

Issue 01/2009

Oxidative Desulfurization-Difluorination of Alkyl Aryl Thioethers:
Synthesis of ω-Substituted 1,1-Difluoroalkanes

Issue 20/2008

Highly Enantioselective Aziridination of N-Protected Imines: Comparison of the Phosphazene EtP2 and Sodium Hydride as Bases

Issue 19/2008

Sequential Aza-Claisen Rearrangement and Ring-Closing Metathesis as a Route to 1-Benzazepine Derivatives

Issue 18/2008

Efficient Chemoenzymatic Synthesis of Phenylacetylrinvanil: An Ultrapotent Capsaicinoid

Issue 17/2008

Investigation of a Tandem Iminium Ion Allylation Approach to Piperidines

Issue 16/2008

Trichlorosilane (HSiCl3) - A Cheap and Convenient Reducing Agent
Synthesis of a xylo-Puromycin Analogue

Issue 15/2008

Reaction of a Polycyclic Diketone with Lithiated Methoxyallene:Synthesis of New Functionalized Cage Compounds

Issue 13/2008

The First Tandem Acetalization/5-exo-dig Cyclization of 6-Phenylethynyl-
pyrimidine-5-carbaldehydes: Efficient Synthesis of 5-Alkoxy-(7Z)-7-benzylidene-5,7-dihydrofuro[3,4-d]pyrimidines

Issue 12/2008

Friedel-Crafts Alkylation of Nitrogen Heterocycles Using [Bmim][OTf] as a Catalyst and Reaction Medium
Copper-Catalyzed Sulfonylation of Arylboronic Acids in Ionic Liquids
Lewis Acid Promoted Oxidative Rearrangement of Tertiary Allylic Alcohols with the PhIO/TEMPO System

Issue 11/2008

Heapy, Amanda M.; Wagner, Thomas W.; Brimble, Margaret M.: Synthesis of the FG Fragment of the Pectenotoxins
Shen, Li; Cao, Song; Liu, Nianjin; Wu, Jingjing; Zhu, Longjie; Qian, Xuhong: Ytterbium(III) Perfluorooctanoate Catalyzed One-Pot, Three-Component Synthesis of Fully Substituted Pyrazoles under Solvent-Free Conditions
Santi, Claudio; Santoro, Stefano; Testaferri, Lorenzo; Tiecco, Marcello: A Simple Zinc-Mediated Preparation of Selenols
Jennequin, Thomas; Labat, Stéphane; Toupet, Loïc; Caille, Jean-Claude; Mauduit, Marc: Stereocontrolled α-Alkylation of Oxime Ether Derived from Terpene: Efficient Synthesis of New Chiral γ- and δ-Amino Alcohols

Issue 07/2008

Iodine-Catalyzed Nucleophilic Substitution Reactions of Benzylic Alcohols

Issue 05/2008

Chankeshwara, Sunay V.: Dimethyl Carbonate (DMC): A Versatile and Environmentally Benign Building Block
Srivastava, Vishnu Prabhakar: Dimethyldioxirane (DMD)
Facile Synthesis of the C1-C13 Fragment of Lyngbouilloside
Microwave-Assisted Reactions of α-Diazosulfoxides to Form α-Oxosulfines

Issue 04/2008

Maity, Annada C.: Selenium Dioxide (SeO2) - A Versatile Reagent
Magalhães de Moreira, Diogo Rodrigo: Lawesson’s Reagent: Endowed With Wide Utility in Organic Synthesis

Issue 20/2007

Wang, Xiaoxia; Zou, Xuefei; Li, Jian; Hu, Qinghong: Efficient Syntheses of β-Amino-N-acylbenzotriazoles and Cinnamides through Regioselective 1,4- or 1,2-Addition of Amines to N-Cinnamoylbenzotriazoles
Kreye, Oliver; Westermann, Bernhard; Wessjohann, Ludger A.: A Stable, Convertible Isonitrile as a Formic Acid Carbanion [-COOH]
Equivalent and Its Application in Multicomponent Reactions

Issue 18/2007

Shi, Da-Qing; Dou, Guo-Lan; Ni, Sai-Nan; Shi, Jing-Wen; Li, Xiao-Yue; Wang, Xiang-Shan; Wu, Hui; Ji, Shun-Jun: A Novel and Efficient Synthesis of 2-Aryl-2H-indazoles via SnCl2-Mediated Cyclization of 2-Nitrobenzylamines

Issue 17/2007

Shibata, Takanori; Fujiwara, Ryo; Takano, Daisuke: Thermal and Au(I)-Catalyzed Intramolecular [4+2] Cycloaddition of Aryl-Substituted 1,6-Diynes for the Synthesis of Biaryl Compounds
Jin, Cheng Hua; Lee, Ho Young; Lee, Sang Hwi; Kim, In Su; Jung, Young Hoon: Direct Etherification of Alkyl Halides by Sodium Hydride in the Presence of N,N-Dimethylformamide

Issue 15/2007

Cecchi, Luca; De Sarlo, Francesco; Machetti, Fabrizio: 4,5-Dihydroisoxazoles by Copper(II)-Catalysed Condensation of Primary Nitroalkanes with Dipolarophiles

Issue 14/2007

Cabello, Noemí; Rodríguez, Cristina; Echavarren, Antonio M.; Jacobs, Jan: Gold-Catalyzed Cyclizations of 1,7-Enynes

Issue 13/2007

Córdova, Armando: One-Pot Organocatalytic Direct Asymmetric Synthesis of γ-AminoAlcohol Derivatives
Jafarzadeh, Mohammad: Trimethylsilyl Azide (TMSN3): A Versatile Reagent in Organic Synthesis

Issue 08/2007

Sridharan, Vellaisamy; Avendaño, Carmen; Menéndez, J. Carlos: General, Mild and Efficient Synthesis of β-Enaminones Catalyzed by Ceric Ammonium Nitrate

Issue 07/2007

Claessens, Sven; Verniest, Guido; Jacobs, Jan; Van Hende, Eva; Habonimana, Pascal; Nguyen Van, Tuyen; Van Puyvelde, Luc; De Kimpe, Norbert; Van Puyvelde, Luc: A Survey of Synthetic Routes towards the Pyranonaphthoquinone Antibiotic Pentalongin and Syntheses of the Corresponding Nitrogen Derivatives

Issue 05/2007

Kazantzi, Georgia; Malamidou-Xenikaki, Elizabeth; Spyroudis, Spyros: Palladium-Catalyzed Allylation of 2-Hydroxy-1,4-naphthoquinone: ­Application to the Preparation of Lapachol

Issue 04/2007

Murthy, A. Sai Krishna; Rambabu, C.; Vijeender, K.; Bhusan, P. Bibhuti; Chandrasekhar, S.: A Pd(OAc)2-Mediated One-Pot Synthesis of Trisubstituted Alkenes via
Michael Addition of a Stabilized Ylide to Baylis-Hillman Adducts

Issue 19/2006

Wang, Jun-Ke; Zong, Ying-Xiao; Yue, Guo-Ren: PEG-Supported Synthesis of 3,5-Disubstituted-1,2,4-Triazoles
Molnár, Árpád; Papp, Attila; Molnár, Á; Papp, A.: Efficient Heterogeneous Palladium-Montmorillonite Catalysts for Heck Coupling of Aryl Bromides and Chlorides
Coquerel, Yoann; Bensa, David; Moret, Vincent; Rodriguez, Jean; Coquerel, Y.; Bensa, D.; Moret, V.; Rodriguez, J.: Synthetic Studies on the MARDi Cascade: Stereoselective Preparation of Sulfonyl-Substituted Seven-Membered Rings

Issue 13/2006

Reddy, Vanga R.: Gold Nanoparticles: Synthesis and Applications

Issue 08/2006

Reich, Nicholas W.; Yang, Cai-Guang; Shi, Zhangjie; He, Chuan; Sun, Nicholas W.: Gold(I)-Catalyzed Synthesis of Dihydrobenzofurans from Aryl Allyl Ethers

Issue 07/2006

Sun, Ya-Ping; Wu, Yikang: An Expeditious Synthesis of Nocardiolactone

Issue 06/2006

Ishihara, Midori; Togo, Hideo: An Efficient Preparation of 2-Imidazolines and Imidazoles from Aldehydes with Molecular Iodine and (Diacetoxyiodo)benzene

Issue 03/2006

Ballini, Roberto; Fiorini, Dennis; Palmieri, Alessandro; Fiorino, Dennis: Highly Convenient, One-Pot Synthesis of Nitriles from Aldehydes Using the NH2OH·HCl/NaI/MeCN System

Issue 19/2005

Godet, Thomas; Bosson, Johann; Belmont, Philippe: Efficient Base-Catalyzed 5-exo-dig Cyclization of Carbonyl Groups on
Unactivated Alkynyl-Quinolines: An Entry to Versatile Oxygenated
Heterocycles Related to the Furoquinoline Alkaloids Family
Prasad, Kavirayani R.; Gholap, Shivajirao L.: An Expeditious Enantiospecific Total Synthesis of (+)-7-epi-Goniofufurone

Issue 12/2005

Mori, Naoshi; Togo, Hideo: Direct Oxidative Conversion of Primary Alcohols to Nitriles Using Molecular Iodine in Ammonia Water
Charette, André B.; Mathieu, Simon; Fournier, Jean-François; Charrette, André B.: Diastereoselective Synthesis of 1,2,3-Substituted Potassium Cyclopropyl Trifluoroborates via an Unusual Zinc-Boron Exchange

Issue 10/2005

Sureshan, Kana M.; Murakami, Tomohiro; Watanabe, Yutaka: Establishment of the Structure of Pinpollitol by Total Synthesis of the Proposed Putative Structure
Patterson, Brian; Rychnovsky, Scott D.: Mukaiyama Aldol-Prins Cyclizations with Ketones

Issue 09/2005

Lohmann, Sophie; Andrews, Stephen P.; Burke, Brenda J.; Smith, Martin D.; Attfield, J. Paul; Tanaka, Hirohisa; Kaneko, Kimiyoshi; Ley, Steven V.: Copper- and Palladium-Containing Perovskites: Catalysts for the Ullmann and Sonogashira Reactions

Issue 08/2005

Ghosh, Rina; Maiti, Swarupananda; Chakraborty, Arijit: One-Pot Multicomponent Synthesis of β-Acetamido Ketones Based on BiCl3 Generated in situ from the Procatalyst BiOCl and Acetyl Chloride

Issue 06/2005

Zhang, G.: Easy Copper-, Ligand- and Amine-Free Sonogashira Coupling Reaction Catalyzed by Palladium on Carbon at Low Catalyst Loading and by Exposure to Air
Dintzner, Matthew R.; Lyons, Thomas W.; Akroush, Michael H.; Wucka, Paul; Rzepka, Adam T.: A Quick, Clean and Green Synthesis of Methylenedioxyprecocene and other Chromenes over Basic Montmorillonite K10 Clay

Issue 01/2005

Wang, Xiao-jun; Xu, Yibo; Zhang, Li; Krishnamurthy, Dhileepkumar; Nummy, Laurence; Farina, Vittorio; Senanayake, Chris H.: A Practical Synthesis of Highly Functionalized Fused 1,6-Dihydroimidazo-[1,2-a]imidazole-2,5-diones, Key Intermediates for LFA-1 Inhibitors

Issue 15/2004

Tararov, Vitali I.; Kadyrov, Renat; Fischer, Christine; Börner, Armin; Bernotas, Ronald C.: Selective N-Benzylation of Amino Acids under Homogeneously Catalyzed Hydrogenation Conditions

Issue 14/2004

Hara, Osamu; Sugimoto, Kazuhiko; Makino, Kazuishi; Hamada, Yasumasa: New Synthesis of a Pyrroloquinoline Skeleton, the Martinelline Core, Using a Tandem Michael-Aldol Strategy
Bernotas, Ronald C.: A Short, Novel Approach to 2,3,4a,5-Tetrahydro-1H-pyrazino[1,2-a]quinoline-4,6-diones

Issue 11/2004

Das, Saibal Kumar: Application of Microwave Irradiation in the Synthesis of Carbohydrates
Shi, Daqing; Wang, Juxian; Shi, Chunling; Rong, Liangce; Zhuang, Oiva; Hu, Hongwen: Synthesis of Quinazolines and Imidazo[1,2-c]quinazolines with the Aid of a Low-Valent Titanium Reagent

Issue 06/2004

Zhao, Pei-Qing; Xu, Li-Wen; Xia, Chun-Gu: Transition Metal-based Lewis Acid Catalyzed Ring Opening of Epoxides Using Amines Under Solvent-Free Conditions
Zhu, C.; Yang, M.; Sun, J.; Zhu, Y.; Pan, Y.: The Synthesis of New C2-Symmetric Chiral 1,4-Diamino Motif and ­Application in Catalytic Asymmetric Alkynylation of meso-Epoxides