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Synthesis 2004(11): 1771-1774
DOI: 10.1055/s-2004-829124
DOI: 10.1055/s-2004-829124
PAPER
© Georg Thieme Verlag Stuttgart · New York
Facile and High-Yielding Preparation of α-Acetoxyphosphonates from α-Hydroxyphosphonates Assisted by Microwave Irradiation
Further Information
Received
16 March 2004
Publication Date:
01 July 2004 (online)
Publication History
Publication Date:
01 July 2004 (online)
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Abstract
A convenient and eco-friendly procedure is described for the efficient preparation of a variety of α-acetyloxyphosphonates from their corresponding α-hydroxyphosphonates using acetic anhydride under microwave irradiation in the absence of solvent.
Key words
hydroxyphosphonates - solvent-free - α-acetyloxyphosphonates - acetic anhydride - microwave irradiation
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