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Synlett 2001; 2001(3): 0418-0420
DOI: 10.1055/s-2001-11417
DOI: 10.1055/s-2001-11417
letter
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Efficient Electrochemical Dicarboxylation of Phenyl-substituted Alkenes: Synthesis of 1-Phenylalkane-1,2-dicarboxylic Acids
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Publication History
Publication Date:
31 December 2001 (online)
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Electrochemical dicarboxylation of phenyl-substituted alkenes in the presence of atmospheric pressure of carbon dioxide with a platinum plate cathode and a magnesium rod anode readily took place efficiently in a DMF solution containing 0.1 M Et4NClO4 to give the corresponding 1,2-dicarboxylic acids in high yields.
carboxylic acids - magnesium - phenyl-substituted alkenes - electrochemical carboxylation - electrochemistry