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Synlett 2000; 2000(8): 1115-1118
DOI: 10.1055/s-2000-6747
DOI: 10.1055/s-2000-6747
letter
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Vilsmeier Reagent for Formylation in Solvent-Free Conditions using Microwaves
Further Information
Publication History
Publication Date:
31 December 2000 (online)
![](https://www.thieme-connect.de/media/synlett/200008/lookinside/thumbnails/10.1055-s-2000-6747-1.jpg)
POCl3-DMF over silica gel has been used for the synthesis of β-chlorovinylaldehydes (1-5), 2-aryl-3-formylindoles (6-8), 2-chloro-3-formylquinolines (9-13) and other aromatic aldehydes (14-20) using solvent-free conditions and microwave irradiation.
microwaves - Vilsmeier reagent - solid-phase synthesis - formylation - aldehydes