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Synlett 2000; 2000(1): 65-66
DOI: 10.1055/s-2000-6452
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Efficient Conversion of Silyl Ethers to Thiocyanates with Ph3P(SCN)2

N. Iranpoor* , H. Firouzabadi, H. Shaterian
  • *Chemistry Department, College of Sciences, Shiraz University, Shiraz 71454, Iran; E-mail: iranpoor@chem.susc.ac.ir
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Publication Date:
31 December 2000 (online)

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A new and efficient method for the conversion of primary and secondary alkyl, aryl, allyl and benzyl silyl ethers to their corresponding thiocyanates by in-situ generation of Ph3P(SCN)2 is described. The reactions occur immediately at room temperature and provide high to excellent yields of thiocyanates.

silyl ethers - thiocyanates - Ph3P(SCN)2

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