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Synlett 1999; 1999(11): 1735-1738
DOI: 10.1055/s-1999-2926
DOI: 10.1055/s-1999-2926
letter
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Synthesis of Perhydrooxazinones from 2-Aza-3-Trimethylsilyloxy-1,3-Butadiene. A General Route to 3,3-Disubstituted-β-Hydroxy Acids
Further Information
Publication History
Publication Date:
31 December 1999 (online)
1-Phenyl-2-aza-3-trimethylsilyloxy-1,3-butadiene reacts with aliphatic, aromatic and cyclic ketones to give in good to excellent yields 6,6-disubstituted-1,3-perhydro-oxazin-4-ones which, in turn, have been readily converted into β-hydroxy carboxylic acids.
Diels-Alder reactions - carboxylic acids - heterocycles - azo compounds