Novel Use of Tetrabutylammonium Borohydride in Ionic Hydrogenation: An Expedient, Mild Method for the Preparation of Alkylferrocenes

Sukanta Bhattacharyya

doi:10.1055/s-1998-1812

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Synlett 1998; 1998(8): 837-838
DOI: 10.1055/s-1998-1812

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Novel Use of Tetrabutylammonium Borohydride in Ionic Hydrogenation: An Expedient, Mild Method for the Preparation of Alkylferrocenes

Sukanta Bhattacharyya^*

^*Department of Chemistry, The University of Mississippi, University, MS 38677, USA

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Publikationsdatum:
31. Dezember 2000 (online)

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NBu₄BH₄ performs the ionic hydrogenation of α-ferrocenyl aldehydes, ketones and alcohols in excellent yields in the presence of zinc chloride. This method allows synthesis of alkylferrocenes with reagent sensitive chromophores and is adaptable to multigram preparations.

NBu₄BH₄ - ionic hydrogenation - α-ferrocenyl - aldehydes - ketones and alcohols - alkylferrocene