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Synlett 1997; 1997(4): 361-362
DOI: 10.1055/s-1997-791
DOI: 10.1055/s-1997-791
letter
© Georg Thieme Verlag, Rüdigerstr. 14, 70469 Stuttgart, Germany. All rights reserved. This journal, including all individual contributions and illustrations published therein, is legally protected by copyright for the duration of the copyright period. Any use, exploitation or commercialization outside the narrow limits set by copyright legislation, without the publisher's consent, is illegal and liable to criminal prosecution. This applies in particular to photostat reproduction, copying, cyclostyling, mimeographing or duplication of any kind, translating, preparation of microfilms, and electronic data processing and storage.
Reactions of Hexamethyldisilathiane with Silyl Acetals: a General Access to Thioformylsilanes
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Publikationsverlauf
Publikationsdatum:
31. Dezember 2000 (online)
![](https://www.thieme-connect.de/media/synlett/199704/lookinside/thumbnails/10.1055-s-1997-791-1.jpg)
Reaction of several silylated acetals with hexamethyldisilathiane (HMDST) in the presence of CoCl2•6H2O affords a simple, novel and general entry to thioformylsilanes, directly trapped in situ as their Diels-alder cycloadducts.
thioformylsilanes - hexamethyldisilathiane - thioaldehydes - silyl acetals - silyl dihydrothiopyrans - Diels-Alder