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Synthesis 1997; 1997(9): 1045-1048
DOI: 10.1055/s-1997-1302
DOI: 10.1055/s-1997-1302
paper
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A Short Efficient Synthesis of 11-Monoacetate of Drimane-8α,11-diol from Norambreinolide
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Publication History
Publication Date:
31 December 2000 (online)
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An efficient two-step synthesis of 11-acetoxydrimane-8α-ol, a valuable intermediate for the synthesis of naturally occurring drimanes, from commercially available norambreinolide, is described. The Baeyer-Villiger oxidation of the initially obtained 8α-hydroxy-12-oxo-11-homodrimane is considered as the key step.
oxidation