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Synlett 1996; 1996(6): 576-578
DOI: 10.1055/s-1996-5481
DOI: 10.1055/s-1996-5481
letter
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Palladium(II)-Catalyzed Dehydrative Cyclization of cis-4-Alkylcycloalken-2-ols. Synthesis of Tricyclic Spiroketals in a One-Pot Sequence
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Publication History
Publication Date:
31 December 2000 (online)
An efficient one-pot process involving palladium-catalyzed dehydrative cyclization, hydroxyl group deprotection and spiroketalization is described and offers an easy access to the tricyclic spiroketal framework of phyllanthocin.
Tetrahydrobenzofurans - spiroketals - palladium catalyst - heterocyclization - diastereoselective - C-O bond formation