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Synlett 1996; 1996(1): 75-78
DOI: 10.1055/s-1996-5321
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A New Strategy for the Synthesis of Selectively Protected Spermidine and Norspermidine Derivatives

Sandrine Lemaire-Audoire, Monique Savignac, Jean-Pierre Genêt*
  • *Laboratoire de Synthèse Organique, CNRS URA 1381, Ecole Nationale Supérieure de Chimie de Paris, 11 rue Pierre et Marie Curie, 75231 Paris Cedex 05, France
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Publikationsdatum:
31. Dezember 2000 (online)

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The synthesis of spermidine derivatives holding three independently removable N-protecting groups has been achieved from diallylamine using the key sequence: selective palladium-catalyzed monodesallylation of diallylamines/N-alkylation.

Polyamine - allylamine - selective desallylation - orthogonal N-protection