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Synlett 1995; 1995(SI): 525-526
DOI: 10.1055/s-1995-5279
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Sonochemical Synthesis of Alkyl Hydroperoxides by Aerobic Reductive Oxygenation of Alkyl Halides

Eiichi Nakamura* , Ken-ichi Sato, Yasuhiro Imanishi
  • *Department of Chemistry, Tokyo Institute of Technology, Meguro, Tokyo 152, Japan
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Publication Date:
31 December 2000 (online)

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Ultrasound irradiation of an aerated solution of an equimolar mixture of an alkyl halide and Bu2t-BuSnH around 0 °C produces the corresponding alkyl hydroperoxide in good yield.

sonochemistry - radical reaction - hydroperoxide - dibutyl-t-butyltin hydride - air