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Synthesis 1994; 1994(9): 901-903
DOI: 10.1055/s-1994-25596
DOI: 10.1055/s-1994-25596
short paper
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Preparation of 2-(6-Carboxyhexyl)- and 2-(6-Methoxycarbonylhexyl)cyclopent-2-en-1-one Using Free Radical Reactions
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Publikationsverlauf
Publikationsdatum:
17. September 2002 (online)
![](https://www.thieme-connect.de/media/synthesis/199409/lookinside/thumbnails/10.1055-s-1994-25596-1.jpg)
Two short and simple synthetic routes to the prostaglandin synthons 2-(6-carboxyhexyl)- and 2-(6-methoxycarbonylhexyl)cyclopent-2-en-1-one have been developed. The first is based on a cyclohexanone oxidative transformation with hydrogen peroxide and di-tert-butyl peroxide, the second on the free radical addition reaction of methyl 9-oxononanoate to acrylaldehyde diacylal.