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Synlett 1994; 1994(7): 485-486
DOI: 10.1055/s-1994-22897
DOI: 10.1055/s-1994-22897
letter
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One Pot Synthesis of Haloacetylenes from Trimethylsilylacetylenes
Further Information
Publication History
Publication Date:
18 September 2002 (online)
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An efficient and convenient method for one step conversion of trimethylsilylacetylenes into haloacetylenes has been developed. This method is sufficiently mild to apply a variety of substrates having many kinds of functional group. The validity of this method is demonstrated in the synthesis of simple model compound of esperamicin/calicheamicin aglycon.