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Synlett 1994; 1994(1): 71-74
DOI: 10.1055/s-1994-22743
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The Intermolecular Diels-Alder Reaction of a 14-membered Diene-Dienophile Pair

Masaya Nakata* , Minoru Yasuda, Shigeru Suzuki, Shigeru Ohba
  • *Department of Applied Chemistry, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama 223, Japan
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Publication Date:
22 March 2002 (online)

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The intermolecular Diels-Alder reaction between methyl 3-oxo-1-cyclotetradecenecarboxylate (5) and (1E,3E)-1-isopropenyl-1,3-cyclotetradecadiene (6) has been investigated. The structures of the adducts under the Et2AICl-promoted conditions and the thermal conditions were determined by 1H NMR and X-ray crystallographic analyses.