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Synthesis 1993; 1993(3): 318-321
DOI: 10.1055/s-1993-25857
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Synthesis of 1,2-Diacylbenzenes from o-Hydroxyaryl Ketone Acylhydrazones Using [(Diacetoxy)iodo]benzene

Robert M. Moriarty* , Bruce A. Berglund, M. Suresh Chander Rao
  • *Department of Chemistry, University of Illinois at Chicago, Box 4348, Chicago, Illinois 60680, USA
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Publikationsdatum:
17. September 2002 (online)

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2′-Hydroxyacetophenone and 2′-hydroxypropiophenone acylhydrazones 3 are oxidized to 1,2-diacylbenzenes 4 using [(diacetoxy)-iodo]benzene in dichloromethane at room temperature in a synthetically useful and high yield reaction.