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Synthesis 1992; 1992(3): 258-260
DOI: 10.1055/s-1992-26081
short paper
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Studies on Organophosphorus Compounds, 53: A New Procedure for the Synthesis of 1-Alkyl or 1-Aryl-1-hydroxy-2-nitroethylphoshonates under PTC Conditions

Chengye Yuan* , Shuhua Cui, Guohong Wang, Hanzhen Feng, Deliang Chen, Chaozhong Li, Yixiang Ding, Ludwig Maier
  • *Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, 345 Lingling Lu, Shanghai 200032, People's Republic of China
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Publication Date:
17 September 2002 (online)

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A series of dialkyl 1-alkyl- or 1-aryl-1-hydroxy-2-nitroethyl-phosphonates and 1-hydroxy-1-(nitromethyl)alkylphosphonates was prepared by nucleophilic addition of nitromethane to dialkyl acylphosphonates in the presence of potassium carbonate and tetrabutylammonium bromide.