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Synthesis 1991; 1991(12): 1147-1150
DOI: 10.1055/s-1991-28407
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N-[1-(Benzotriazol-1-yl)alkyl]amides, Versatile Amidoalkylation Reagents. Part 3.1 Syntheses of Open-Chain N-Protected-Hemithioaminals

Alan R. Katritzky* , Ichiro Takahashi, Wei-Qiang Fan, Juliusz Pernak
  • *Department of Chemistry, University of Florida, Gainesville, FL 32611-2046, USA
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Publication Date:
29 April 2002 (online)

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N-[(1-Benzotriazol-1-yl)alkyl]amides 1 react readily with a variety of thiols (both aliphatic and aromatic) and sodium sulfide under mild conditions to give N-acylhemithioaminals in good yields.