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Synlett 1991; 1991(6): 435-438
DOI: 10.1055/s-1991-20755
DOI: 10.1055/s-1991-20755
letter
© Georg Thieme Verlag, Rüdigerstr. 14, 70469 Stuttgart, Germany. All rights reserved. This journal, including all individual contributions and illustrations published therein, is legally protected by copyright for the duration of the copyright period. Any use, exploitation or commercialization outside the narrow limits set by copyright legislation, without the publisher's consent, is illegal and liable to criminal prosecution. This applies in particular to photostat reproduction, copying, cyclostyling, mimeographing or duplication of any kind, translating, preparation of microfilms, and electronic data processing and storage.
Radical Deoxygenaton of Secondary and Primary Alcohols with Phenylsilane
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Publikationsverlauf
Publikationsdatum:
07. März 2002 (online)
Thionocarbonates and xanthates formed from secondary and primary alcohols are easily deoxygenated in 85-100% yield by radical deoxygenation with phenylsilane and 2,2′ -azobisisobutyronitrile or benzoyl peroxide in boiling toluene.