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Synthesis 1990; 1990(4): 333-336
DOI: 10.1055/s-1990-26869
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Reduction of Allylic Nitro Compounds to Oximes with Carbon Disulfide under Solid-liquid Phase-Transfer Catalysis Conditions

Domenico Albanese* , Dario Landini, Michele Penso
  • *Centro C.N.R. and Dipartimento di Chimica Organica e Industriale dell' Università, Via Golgi 19, I-20133 Milano, Italy
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Publication Date:
17 September 2002 (online)

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A mild procedure for the synthesis of allylic oximes 2 from the corresponding nitro derivatives 1, using carbon disulfide as reducing agent in the presence of wet potassium carbonate and a catalytic amount of a phase-transfer agent, is described.