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Synthesis 1989; 1989(3): 175-178
DOI: 10.1055/s-1989-27185
DOI: 10.1055/s-1989-27185
paper
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Cleavage of Isoxazolines with Tricarbonyltris(acetonitrile)molybdenum and Silica Gel. Synthesis of 1-(2-Oxoalkyl)cyclopropanols from lsoxazoline-5-spirocyclopropanes
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Publication History
Publication Date:
17 September 2002 (online)
An efficient synthesis of 1-(2-oxoalkyl)cyclopropanols [or (1-hydroxycyclopropyl)methyl ketones] from isoxazoline-5-spirocyclopropanes by selective N-O cleavage effected by Mo(CO)3(MeCN)3 and silica gel is described.