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Synthesis 1986; 1986(9): 762-763
DOI: 10.1055/s-1986-31768
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Alkylation Studies; Part II1: Bis-alkylation of Diethyl Cyanomethanephosphonate

Rajendra K. Singh*
  • *Monsanto Agricultural Company, 800 North Lindbergh Blvd., St. Louis, Missouri 63167 U. S. A.
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Publication Date:
20 August 2002 (online)

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A convenient high-yield method for the geminal dialkylation of diethyl cyanomethanephosphonate with alkyl halides under ion-pair extraction conditions is described.