PDF herunterladen
Synthesis 1985; 1985(8): 754-755
DOI: 10.1055/s-1985-31333
communication
© Georg Thieme Verlag, Rüdigerstr. 14, 70469 Stuttgart, Germany. All rights reserved. This journal, including all individual contributions and illustrations published therein, is legally protected by copyright for the duration of the copyright period. Any use, exploitation or commercialization outside the narrow limits set by copyright legislation, without the publisher's consent, is illegal and liable to criminal prosecution. This applies in particular to photostat reproduction, copying, cyclostyling, mimeographing or duplication of any kind, translating, preparation of microfilms, and electronic data processing and storage.

Large Scale Synthesis of 2-Fluoroacrolein

H. Molines* , T. Nguyen, C. Wakselman
  • *CNRS-CERCOA 2 à 8 Rue Henri Dunant, F-94320 Thiais, France
Weitere Informationen

Publikationsverlauf

Publikationsdatum:
17. September 2002 (online)

  als PDF herunterladen  Lizenzen und Reprints Alle Artikel dieser Rubrik

A large scale preparation of 2-fluoroacrolein (1) is achieved by refluxing the cyclopropyl ether (5), prepared by the addition of chlorofluorocarbene (3) to n-butyl vinyl ether (2), in n-butanol/pyridine mixture and subsequently bydrolysing the acetal 7 formed.