Synthesis 2014; 46(11): 1511-1517
DOI: 10.1055/s-0033-1340978
paper
© Georg Thieme Verlag Stuttgart · New York

Microwave-Assisted Synthesis of Biotin Conjugates with Quinolone Antibiotics via Amino Acids

Siva S. Panda
a   Center for Heterocyclic Compounds, Department of Chemistry, University of Florida, Gainesville, FL 32611-7200, USA   Fax: +1(352)3929199   eMail: panda@chem.ufl.edu   eMail: katritzky@chem.ufl.edu
,
Roman N. Naumov
a   Center for Heterocyclic Compounds, Department of Chemistry, University of Florida, Gainesville, FL 32611-7200, USA   Fax: +1(352)3929199   eMail: panda@chem.ufl.edu   eMail: katritzky@chem.ufl.edu
,
Abdullah M. Asiri
b   Chemistry Department, King Abdulaziz University, Jeddah 21589, Saudi Arabia
c   Center for Advanced Materials Research (CEAMR), King Abdulaziz University, Jeddah 21589, Saudi Arabia
,
Alan R. Katritzky*
a   Center for Heterocyclic Compounds, Department of Chemistry, University of Florida, Gainesville, FL 32611-7200, USA   Fax: +1(352)3929199   eMail: panda@chem.ufl.edu   eMail: katritzky@chem.ufl.edu
b   Chemistry Department, King Abdulaziz University, Jeddah 21589, Saudi Arabia
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Publikationsverlauf

Received: 06. Januar 2014

Accepted after revision: 20. Februar 2014

Publikationsdatum:
02. April 2014 (online)


Abstract

Benzotriazole-activated biotin was utilized as a versatile building block for the efficient and convenient synthesis of novel biotin conjugates with quinolone antibiotics via amino acid linkers under microwave irradiation. The products are obtained in yields of 70–91% with retention of chirality.

Supporting Information

 
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